Held synthesized the acid from ethyl chlor-acetoacetate (from chlorine and acetoacetic ester) by heating with potassium cyanide and saponifying the resulting nitrile.
The process of manufacturing soaps by boiling fatty acids with caustic alkalis or sodium carbonate came into practice with the development of the manufacture of candles by saponifying fats, for it provided a means whereby the oleic acid, which is valueless for candle making, could be worked up. The combination is effected in open vats heated by a steam coil and provided with a stirring appliance; if soda ash be used it is necessary to guard against boiling over.
The first is carried out by saponifying the soap with acid in the heat when the fatty acids come to the surface.
Distillation in a vacuum is practised in two forms: - if the pump draws off steam as well as air it is termed a "wet" air-pump; if it only draws off air, it is a "dry" air-pump. In the glycerin industry the lyes obtained by saponifying the fats are first evaporated with "wet vacuum" and finally distilled with closed and live steam and a "dry vacuum."
The conversion of the mixture obtained by extracting coca-leaves into cocaine is effected by saponifying the esters into ecgonine and the respective acids, and then benzoylating and methylating the ecgonine.
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